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Park, Cheol-Min
Synthetic & Medicinal Chemistry Lab
Research Interests
  • Organic synthesis, medicinal chemistry, chemical biology

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Electrosynthesis of Dihydropyrano[4,3‐b ]indoles Based on a Double Oxidative [3+3] Cycloaddition

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Title
Electrosynthesis of Dihydropyrano[4,3‐b ]indoles Based on a Double Oxidative [3+3] Cycloaddition
Author
Choi, SubinPark, JinhwiYu, EunsooSim, JeongwooPark, Cheol-Min
Issue Date
2020-05
Publisher
WILEY-V C H VERLAG GMBH
Citation
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Abstract
Oxidative [3+3] cycloadditions offer an efficient route for six-membered-ring formation. This approach has been realized based on an electrochemical oxidative coupling of indoles/enamines with active methylene compounds followed by tandem 6 pi-electrocyclization leading to the synthesis of dihydropyrano[4,3-b]indoles and 2,3-dihydrofurans. The radical-radical cross-coupling of the radical species generated by anodic oxidation combined with the cathodic generation of the base from O-2 allows for mild reaction conditions for the synthesis of structurally complex heterocycles.
URI
https://scholarworks.unist.ac.kr/handle/201301/32301
URL
https://onlinelibrary.wiley.com/doi/full/10.1002/ange.202003364
DOI
10.1002/ange.202003364
ISSN
1433-7851
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PHY_Journal Papers
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