File Download
There are no files associated with this item.
SFX Link
- Find it @ UNIST can give you direct access to the published full text of this article. (UNISTARs only)
- Seok, Sang Il
- Laboratory for Energy Harvesting Materials and Systems
Views & Downloads
Detailed Information
Cited time in 
Cited time in 
Cited time in
Metadata Downloads
High-yield synthesis of quantum-confined CdS nanorods using a new dimeric cadmium(II) complex of S-benzyldithiocarbazate as single-source molecular precursor
- Author(s)
- Bera, Pulakesh, Kim, Chong-Hyeak, Seok, Sang Il
- Issued Date
- 2010-04
- Citation
- SOLID STATE SCIENCES, v.12, no.4, pp.532 - 535
- Abstract
- A convenient solvothermal single-source route has been developed for the bulk synthesis of CdS nanorods using new air stable dimeric cadmium(II) complex of S-benzyldithiocarbazate, [Cd(PhCH(2)SC(=S)NHNH(2))Cl(2)](2), at a relatively low temperature. The decomposition of the precursor was made by heating at 160 degrees C in hexamethylenediamine (HMDA) to give amine capped CdS nanocrystals having yield ca. 90%; nano-dimensional rods are clearly visible in transmission electron microscope (TEM). The nanorods have been further characterized by X-ray diffraction (XRD), energy dispersed X-ray spectroscopy (EDX), FTIR and optical measurements. The structure of precursor was also established by single crystal X-ray crystallography. (C) 2009 Elsevier Masson SAS. All rights reserved
- Publisher
- ELSEVIER SCIENCE BV
- ISSN
- 1293-2558
Items in Repository are protected by copyright, with all rights reserved, unless otherwise indicated.