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Baek, Jong-Beom
Center for Dimension-Controllable Organic Frameworks
Research Interests
  • Covalent Organic Frameworks (COFs), Carbon Nanotubes(CNTs), graphene, Energy Conversion and Storage

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Synthesis of Saddle-Shape Octaaminotetraphenylene Octahydrochloride

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Title
Synthesis of Saddle-Shape Octaaminotetraphenylene Octahydrochloride
Author
Ahmad, IshfaqKim, DongwookKodirov, RukhilloYu, Soo-YoungSeo, Jeong-MinMahmood, JaveedBaek, Jong-Beom
Issue Date
2021-11
Publisher
AMER CHEMICAL SOC
Citation
JOURNAL OF ORGANIC CHEMISTRY, v.86, no.21, pp.14398 - 14403
Abstract
Apart from being experimentally and theoretically interesting, tetraphenylene has potential applications in different fields, including supramolecular chemistry, material science, and asymmetric catalysis. Although a wide range of substituted tetraphenylenes have been reported, octaamine-based tetraphenylene derivatives have not been reported because of their instability. Here, stable octaaminotetraphenylene octahydrochloride is synthesized from the bromination of tetraphenylene to octabromotetraphenylene, which is subsequently aminated into octaiminotetraphenylene. Finally, the imino derivative is deprotected to yield octaaminotetraphenylene octahydrochloride.
URI
https://scholarworks.unist.ac.kr/handle/201301/55335
URL
https://pubs.acs.org/doi/10.1021/acs.joc.1c01127
DOI
10.1021/acs.joc.1c01127
ISSN
0022-3263
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ECHE_Journal Papers
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