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Lah, Myoung Soo
Nanoporous Materials Lab
Research Interests
  • Metal-Organic Frameworks (MOFs)

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Scalable Synthesis of Pure and Stable Hexaaminobenzene Trihydrochloride

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Title
Scalable Synthesis of Pure and Stable Hexaaminobenzene Trihydrochloride
Author
Lah, Myoung SooBaek, Jong-BeomMahmood, JaveedKim, DongwookJeon, In-Yup
Keywords
hexaaminobenzene - palladium - reduction - TATB - TNA
Issue Date
201301
Publisher
GEORG THIEME VERLAG KG
Citation
SYNLETT, v.24, no.2, pp.246 - 248
Abstract
Synthesis of hexaaminobenzene (HAB) in pure and stable form has remained as an important challenge for a long time, since it is a fascinating synthon for the synthesis of aromatic nitrogenous compounds having many interesting applications. Here, we report an improved synthesis of pure and stable HAB form using modified catalytic hydrogenation in aqueous acidic medium. The structure of needle-shaped HAB crystals was confirmed by single-crystal X-ray diffraction study. The synthetic protocol could thus be a simple, but efficient for the large-scale synthesis of highly pure and stable HAB.
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DOI
http://dx.doi.org/10.1055/s-0032-1317696
ISSN
0936-5214
Appears in Collections:
ECHE_Journal Papers

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