Preparation of silica nanospheres and porous polymer membranes with controlled morphologies via nanophase separation
Cited 0 times inCited 0 times in
- Preparation of silica nanospheres and porous polymer membranes with controlled morphologies via nanophase separation
- Lee, Jung-Pil; Choi, Sinho; Park, Soojin
- Carbon source; Carbonization process; Controlled morphology; Different structure; In-situ; Matrix components; Mixing ratios; Nano scale; Nanophase separation; Polymer content; Porous carbons; Porous polymers; Random network; Silica beads; Silica nanospheres; Silica sols; Silica Sphere; Silica structures; Tetraorthosilicate
- Issue Date
- NANOSCALE RESEARCH LETTERS, v.7, no., pp. -
- We successfully synthesized two different structures, silica nanospheres and porous polymer membranes, via nanophase separation, based on a sol-gel process. Silica sol, which was in situ polymerized from tetraorthosilicate, was used as a precursor. Subsequently, it was mixed with a polymer that was used as a matrix component. It was observed that nanophase separation occurred after the mixing of polymer with silica sol and subsequent evaporation of solvents, resulting in organizing various structures, from random network silica structures to silica spheres. In particular, silica nanospheres were produced by manipulating the mixing ratio of polymer to silica sol. The size of silica beads was gradually changed from micro- to nanoscale, depending on the polymer content. At the same time, porous polymer membranes were generated by removing the silica component with hydrofluoric acid. Furthermore, porous carbon membranes were produced using carbon source polymer through the carbonization process.
- ; Go to Link
Appears in Collections:
- ECHE_Journal Papers
- Files in This Item:
can give you direct access to the published full text of this article. (UNISTARs only)
Show full item record
Items in DSpace are protected by copyright, with all rights reserved, unless otherwise indicated.