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Preparation of Cu2ZnSnS4 thin films via electrochemical deposition and rapid thermal annealing

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Title
Preparation of Cu2ZnSnS4 thin films via electrochemical deposition and rapid thermal annealing
Author
Lee, Kee DooSeo, Se-WonLee, Doh-KwonKim, HonggonJeong, Jeung-HyunKo, Min JaeKim, BongSooKim, Dong HwanKim, Jin Young
Keywords
Thin film solar cell;  Electrochemical deposition;  RTA;  Sulfurization
Issue Date
201311
Publisher
ELSEVIER SCIENCE SA
Citation
THIN SOLID FILMS, v.546, no., pp.294 - 298
Abstract
We fabricated metallic Cu-Zn-Sn (CZT) precursor thin films via electrochemical deposition from aqueous metal salt solution on Mo-coated soda-lime glass substrates, and the influence of the subsequent sulfurization condition on the morphology, composition and structure of the final Cu2ZnSnS4 (CZTS) thin films was investigated. A rapid thermal annealing equipment was used for a systematic control of the sulfurization process parameters. The as-deposited films are composed of binary metallic alloys, which can be converted to the highly crystalline CZTS phase after sulfurization at temperatures above 500 degrees C. The composition of the CZT film barely changes during the sulfurization, and a small amount of CuS-based secondary phases exists even at 550 degrees C. However, a quick post-annealing KCN treatment effectively and selectively removes the secondary phase, evidenced by the Raman spectroscopy and elemental.
URI
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DOI
http://dx.doi.org/10.1016/j.tsf.2013.02.051
ISSN
0040-6090
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SNS_Journal Papers
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