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Seok, Sang Il
Laboratory for Energy Harvesting Materials and Systems
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Colloidal synthesis of octahedral shaped PbSe nanocrystals from lead oleate and Se : Temperature effect

Author(s)
Gokarna, AnishaJung, Ki-WonKhanna, PKBaeg, Jin-OokSeok, Sang Il
Issued Date
2005-11
DOI
10.5012/bkcs.2005.26.11.1803
URI
https://scholarworks.unist.ac.kr/handle/201301/18689
Fulltext
http://koreascience.or.kr/article/ArticleFullRecord.jsp?cn=JCGMCS_2005_v26n11_1803
Citation
BULLETIN OF THE KOREAN CHEMICAL SOCIETY, v.26, no.11, pp.1803 - 1806
Abstract
Formation of octahedral shaped PbSe quantum dots at higher synthesis temperature is being reported in this paper. The synthesis includes the reaction between lead oleate and trioctylphosphine selenide under inert gas conditions to produce PbSe. TEM, SEM, XRD and EDS were used to characterize the samples. The SEM exhibited the formation of spherical shaped nanocrystals at temperature below 140 degrees C and octahedral shaped nanoparticles at higher temperatures. Moreover, the TEM also showed the well resolved (111) lattice fringes proving that the nanocrystals were crystalline in nature. Synthesis of highly pure PbSe nanocrystals was another interesting aspect of this research
Publisher
KOREAN CHEMICAL SOC
ISSN
1229-5949
Keyword (Author)
octahedral PbSenanocrystalscolloidal synthesistemperature effectslead oleate
Keyword
ASSEMBLIESMONOLAYERSDIODESLIGHT

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